Technical Research Services > Available teams > Single-crystal X-ray Diffraction (XRD)
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Research Technical Services

Diffraction of X-rays of Monocristall

DRXM

It Technique of Raigs-X de Monocristall he uses itself for the structural determination from a crystal. That is, the threedimensional image is obtained from the molecule or molecules that form the crystal, being able to establish itself clearly which it is its structure, you separate them and angles of link, configurations, links for bridge of hydrogen, etc.

Job request

In order to request it the order form has to be filled in and make it arrive at the staff of the Chemical and Structural Unit of Analysis

It be necessary to inform of the toxicity and of the precautions of storage. Once the report given, there is a maximum deadline  of a week to pick up the sample, but this will be destroyed.

The equipment

Difractòmetre de Raigs X of Monocrystal:

Brand:
Bruker


Model:
D8 QUEST ECHO
Technical specifications:
  • Tube of X-Ray of Molybdenum
  • Detector of Area PHOTON II (type CPAD)
  • Goniometer of three circles
  • It can work at temperature no environment of 80ºC to -173ºC (OXFORD Cryostream 800)

How does it work?

Necesaria is a crystalline sample, of which a crystal is selected that is used to make the acquisition of data of its pattern of diffraction. These sleep data handled with the suitable software in order to solve and make the refinement of the structure.

Applications / Practical cases

 Chemical, Pharmaceutical industry and Biotechnology. Identification of Substances. Studies of Polymorphism.

More information:

More information:

Organisations that have funded the acquisition of the team:

European Union. European background of regional development.
Ministerio de Economia, Industria y Competitividad. UNGI15-EE-3839

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