Capacitat per analitzar críticament a partir de la recollida d'informació i la interpretació de dades , situacions complexes i dissenyar estratègies creatives i innovadores per resoldre-les Saber comunicar-se oralment i per escrit en l'àmbit científic i professional , utilitzant les llengües pròpies i l'anglès Treballar en equip contribuint a l'elaboració de projectes específics i multidisciplinaris Aplicar processos metrològics per a l'obtenció d'informació de qualitat en la resolució de problemes qualitatius i quantitatius relacionats amb la identificació , caracterització i determinació de substàncies orgàniques i inorgàniques
1. Structure determination of organic and organometal·lic compounds: fundamentals and basic concepts 2. Mass spectrometry (MS): Ionization techniques. Mass analyzers. Fragmentation mechanisms. Tandem mass spectrometry. Applications and examples 3. Nuclear Magnetic Resonance Spectroscopy (NMR): NMR spectroscopy and molecular structure. NMR spectroscopy of "other" nuclei. Bidimensional NMR
Tipus d’activitat Hores amb professor Hores sense professor Total Anàlisi / estudi de casos 4,00 13,00 17,00 Prova d'avaluació 4,00 0 4,00 Sessió expositiva 8,00 17,00 25,00 Sessió participativa 12,00 17,00 29,00 Total 28,00 47,00 75
Schalley, Christoph A (cop. 2009 ). Mass spectrometry and gas-phase chemistry of non-covalent complexes . Hoboken: Wiley. Catàleg Cole, Richard B. (cop. 1997 ). Electrospray ionization mass spectrometry : fundamentals,instrumentation, and applications . New York [etc.]: Wiley-Interscience. Catàleg Gross, Jürgen H (2004 ). Mass spectrometry : a textbook . Berlin: Springer. Catàleg Hesse, Manfred (1996 ). Spectroscopic methods in organic chemistry . New York: Georg Thieme. Catàleg Silverstein, Robert M (1998 ). Spectrometric identification of organic compounds (6th ed.). New York: John Wiley. Catàleg Jacobsen, Neil E (2007 ). NMR spectroscopy explained : simplified theory, applications and examples for organic chemistry and structural biology . Hoboken: John Wiley. Catàleg Balci, Metin (2005 ). Basic 1H- and 13C-NMR spectroscopy . Amsterdam [etc.]: Elsevier. Catàleg Mitchell, Terence N (2004 ). NMR - from spectra to structures : an experimental approach . Berlin [etc.]: Springer. Catàleg Günther, Harald (cop. 1995 ). NMR spectroscopy : basic principles, concepts, and applications in chemistry (2nd ed.). Chichester [etc.]: John Wiley & Sons. Catàleg Suryanarayana, C (1998 ). X-Ray Diffraction : a practical approach . New York: Plenum Press. Catàleg
Activitats d'avaluació: Descripció de l'activitat Avaluació de l'activitat % Problem-solving exercises: group exercises related to the syllabus will periodically be performed in class This activity cannot be repeated. In making these exercises comprehension of the exercise, clarity of writing, use of correct terminology, and the correction of the answer will be taken into account. 30 Final examination: this will consist of applied questions and problems from the whole of the syllabus This activity can be repeated. The examination will consist of applied questions and problems from the whole of the syllabus. In making the examination the correct approach to the solution of the problems, the full description of the data and the correction of the answer will be taken into account 70
During the course continuous evaluation exercises will be performed in class. Failure to attend any of the evaluation exercises will result in a zero for the corresponding part of the total mark. The subject will only be qualified as "No presentat" when the student has not attended any of the evaluation exercises or has only attended the first problem-solving exercise (see the specific criteria for the qualification of "No presentat"). The minimum pass mark will be 4 out of 10 in the final exam and an overall mark of 5 out of 10. Activities that can be repeated: Only the final examination can be repeated. In the case that a student repeats the final examination the new mark will substitute the old mark independently of whether this represents an improvement. Students wishing to repeat the final examination must notify the lecturer at least one week before the official date for resits. Criteris específics de la nota «No Presentat»:The subject will only be qualified as "No Presentat" when the student has not attended any of the evaluation exercises or has only attended the first problem-solving exercise.
It is necessary to have previous knowledge on structural determination techniques (MS and NMR) to follow the course.