Dades generals

Curs acadèmic:
2017
Descripció:
Laboratori integrat sobre mètodes analítics
Crèdits ECTS:
3

Grups

Grup A

Durada:
Semestral, 1r semestre
Professorat:
NURIA FIOL SANTALO
Idioma de les classes:
Anglès (100%)

Competències

  • CT08 Planificar i organitzar les propostes i projectes
  • CT12 Avaluar la sostenibilitat de les propostes i actuacions pròpies
  • CT15 Utilitzar la llengua anglesa
  • CE23 Capacitat per a l'anàlisi, disseny, simulació i optimització de processos i productes

Continguts

1. Revision of the basic principles of the good practices, the use of glass material, safety, environment protection, etc in the laboratory of chemistry.

2. Preparation of solutions and reagents necessary to perform the programmed laboratory experiences.

3. Experience 1. Introduction to different analytical methods of Molecular Spectroscopy.

4. Experience 2. Introduction to quantitative analysis using Molecular Spectroscopy.

5. Experience 3. Introduction to quantitative analysis using Atomic Absortion Spectroscopy.

6. Experience 4. Introduction to qualitative and quantitative analysis using Gas Chromatography.

7. Experience 5. Introduction to qualitative and quantitative analysis using HPLC Chromatography.

8. Design and development of an integrated laboratory experience (ILE). Products synthesis; qualitative and quantitative analysis of different analytes by different spectroscopic and chromatographic techniques.

Activitats

Tipus d’activitat Hores amb professor Hores sense professor Total
Altres 2 2 4
Classes pràctiques 18 14 32
Elaboració de treballs 4 3 7
Prova d'avaluació 3 3 6
Resolució d'exercicis 0 6 6
Treball en equip 4 16 20
Total 31 44 75

Bibliografia

  • Dunnivant, Frank M (2004 ). Environmental laboratory exercices for instrumental analysis and environmental chemistry . Hoboken, N.J.: John Wiley & Sons. Catàleg
  • Skoog, Douglas A (cop. 2001 ). Principios de análisis instrumental (5ª ed.). Madrid [etc.]: McGraw-Hill. Catàleg
  • Vogel, Arthur Israel (2000). Vogel's text book of quantitative chemical analysis. Person Education. Catàleg
  • Rouessac, Francis (2000). Chemical analysis: modern instrumental methods and techniques. John Wiley. Catàleg
  • Vogel, Arthur Israel (1961 ). A Text-book of quantitative inorganic analysis : including elementary instrumental analysis (3rd. ed.). London: Longmans. Catàleg

Avaluació i qualificació

Activitats d'avaluació:

Descripció de l'activitat Avaluació de l'activitat %
Experience 1 report In the laboratory, the accuracy of the calculations to make the solutions, the appropriate manipulation of the reagents and glass material and a proper laboratory note book maintenance are evaluated. The individual experience report is evaluated taking into account the writing and the accuracy of the obtained results as well as the answers to the proposed questions. 3
Experience 2 report In the laboratory, the accuracy of the calculations to make the solutions, the appropriate manipulation of the reagents and glass material and a proper laboratory note book maintenance are evaluated. The individual experience report is evaluated taking into account the writing and the accuracy of the obtained results as well as the answers to the proposed questions. 3
Experience 3 report In the laboratory, the accuracy of the calculations to make the solutions, the appropriate manipulation of the reagents and glass material and a proper laboratory note book maintenance are evaluated. The individual experience report is evaluated taking into account the writing and the accuracy of the obtained results as well as the answers to the proposed questions. 3
Experience 4 report In the laboratory, the accuracy of the calculations to make the solutions, the appropriate manipulation of the reagents and glass material and a proper laboratory note book maintenance are evaluated. The individual experience report is evaluated taking into account the writing and the accuracy of the obtained results as well as the answers to the proposed questions. 3
Experience 5 report In the laboratory, the accuracy of the calculations to make the solutions, the appropriate manipulation of the reagents and glass material and a proper laboratory note book maintenance are evaluated. The individual experience report is evaluated taking into account the writing and the accuracy of the obtained results as well as the answers to the proposed questions. 3
Experiences questionnaires Once finished each laboratory experience the students must answer several questions concerning the experience. Each question has three answers and they have just one attempt to provide the right answer. These questionnaires must be filled up during the week after the corresponding experience is performed in the laboratory. The questionnaires are activated for one week. The Moodle platform make an automatic evaluation of the questionnaires answers. 15
Integrated laboratory experience (ILE) The difficulty of the objectives and the planned activities for the development of the study will be evaluated. In the laboratory the correctness of the methodology and calculations will be evaluated. 15
Integrated Laboratory Experience report (ILE) The report of the study carried out corresponding to ILE must be presented in format of scientific article. The different sections, introduction, objectives, experimental, results and discussion and conclusions will be evaluated. 15
Final exam At the end of the semester, the students will be evaluated in a written test. The correction of the responses as well as the steps and discussion to solve exercises and get the right solution will be evaluated. Also, the clarity and correction both in oral and written communication. 40

Qualificació

Students will be evaluated on the following:
Laboratory experiences reports 15%
Experiences questionnaires 15%
Integrated Laboratory Experience development(ILE) 15%
Integrated Laboratory Experience report (ILE) 15%
Final exam 40% (when the exam scores are equal or higher than 5/10)
Attention: The activities have a unique evaluation. Only the final exam coul be reapeated.

Criteris específics de la nota «No Presentat»:
A student can only be considered "non evaluated" when he/her has not participated in any of the evaluations activities after 1th of april 2018.

Observacions

És imprescindible tenir aprovada o convalidada l'assignatura de Tècniques Instrumentals d'Anàlisi Química o bé cursar-la en el mateix semestre que Experimentació en Química II.

Assignatures recomanades

  • Tècniques instrumentals d'anàlisi química